trace analytics
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standard services

 

Servicing clients throughout the United States, Trace Analytical Laboratories, Inc. (Trace), is a leading independent environmental testing laboratory. Trace is dedicated to providing prompt, accurate analysis of potential contaminants in water, air, soil, sludge, hazardous waste, and sediment.

We are committed to the quality, traceability, and defensibility of data. Trace's Quality Assurance/Quality Control Program is centered around this commitment. All records are complete and retrievable. Trace works with its clients from initial project planning through final report preparation and interpretation. The quality of the data provides a greater benefit to the client when the laboratory is involved in project analytical needs.

Trace is accredited by the National Environmental Laboratory Accrediation Program (NELAP) and provides analytical services in compliance with the requirements of the Department of Defense Quality Systems Manual for Environmental Laboratories to support Department of Defense projects (e.g. USACE, AFCEE, U.S. Navy).

Trace services include organic, inorganic, and metals analyses in support of CERCLA, SARA, RCRA, SDWA, CWA, the Clean Air Act, and other EPA regulatory programs.

Mobile laboratory services are also provided by Trace. Our mobile laboratory uses standard laboratory instrumentation and can analyze for any compounds under method SW-846, 8260, or EPA 624. Trace's mobile laboratory can provide the client with on-site screening or laboratory-quality data.

Quality Assurance/Quality Control
Trace follows a formal, written, Quality Assurance/Quality Control program which meets or exceeds EPA guidelines. We also participate in the EPA's Water Pollution (WP) and Water Supply (WS) proficiency testing programs. 

Turnaround Times
Standard turnaround time is 5 - 10 business days for most projects. Larger, more complex projects may have longer turnaround times of 2 - 3 weeks. Faster turnaround times may be possible depending on the availability of laboratory resources and the project scope. Please call the laboratory to request a rush turnaround time before sample submission.

Certifications
Trace is accredited by the National Environmental Laboratory Accreditation Program (NELAP) and holds certifications from the Michigan Department of Environmental Quality and the State of Wisconsin.

Data Reporting

Level I

This report includes tabulated results, receipt and analyses dates, method numbers, sample descriptions, detection limits, and qualifiers (if needed).

Level II

This report includes all items from the Level I report and adds results of internal batch Quality Control (QC) analyses associated with the samples. The QC results include surrogate recoveries, matrix spike, method blanks, and laboratory control samples.

Level III

This report includes all items from the Level II report and adds raw data.

Level IV

This report includes all items from the Level III report and adds CLP-like forms where applicable.

Sample containers
Sample containers, coolers, labels, custody seals, trip blanks, temperature blanks, chain-of-custody forms and shipment to the client via UPS Ground are included in Trace's fees. If a client requests next day shipping, the client is responsible for those charges.

Sample disposal
Samples are retained for 45 days. Samples are disposed of at the end of 45 days unless advance arrangements are made with Trace for sample return, or a longer storage time.
 

Test Method
References
General chemistry parameters back to top
Asbestos EPA 600 / R-93 / 116
Alkalinity SM 2320-B
Ammonia Nitrogen EPA 350.1
Adsorbable Organic Halides, (AOX) EPA 1650
Biochemical Oxygen Demand, (BOD) SM 5210-B
Bromide EPA 300.0
BTU content ASTM D240
Carbon Dioxide SM 4500-CO2 B
Chemical Oxygen Demand, (COD) EPA 410.4 Plumb Method for Soil
Chloride SM 4500-Cl- D / EPA 300.0
Chlorine EPA 330.5
Conductivity EPA 120.1
Cyanide, Total EPA 335.4 / 9012
Cyanide, Amenable EPA 335.1 / 9012
Cyanide, Available EPA OIA-1677
Extractable Organic Halides, (EOX) EPA 9023
Flash Point EPA 1010
Fluoride EPA 300.0
Formaldehyde AOAC 31.203
Fraction of Organic Carbon, (FOC) ASTM D2974
Grain Size w/o Hydrometer ASTM D1140
Grain Size w/ Hydrometer ASTM D422
Hardness SM 2340 B / EPA 130.2
Hydrogen Peroxide EM Science Reflectoquant
Nitrate Nitrogen EPA 300.0
Nitrate/Nitrite Nitrogen EPA 353.2 / 300.0
Nitrite Nitrogen EPA 300.0
Nitrogen, Total Kjeldahl, (TKN) EPA 351.2
Oil and Grease EPA 413.1
Oil and Grease (HEM) EPA 1664A
Orthophosphate EPA 365.1
Oxygen, Dissolved SM 4500-O-C & G
Paint Filter EPA 9095
pH EPA 150.1
Percent Solids ASTM D2974
Phenolics, Total EPA 420.1
Phosphorus, Total EPA 365.1 / 6010 / 200.7
Solids, Dissolved SM 2540-C
Solids, Suspended SM 2540-D
Solids, Total SM 2540-B
Solids, Volatile EPA 160.4
Specific Gravity, (Density) - Water SM 2710 F
Specific Gravity, (Density) - Solid ASTM D854
Sulfate EPA 300.0
Sulfide EPA 376.1 / 376.2
Sulfide, (for leather processing effluents) 40CFR, Part 425
Sulfite EPA 377.1
Surfactants, (MBAS) SM 5540-C
Tannin and Lignin SM 5550 B
Total Organic Carbon, (TOC) - Water SM 5310-D / 9060
Total Organic Carbon, (TOC) - Solid Walkey - Black
Total Organic Halides, (TOX) EPA 9020
Total Petroleum Hydrocarbons, (TPH) EPA 418.1
Turbidity EPA 180.1
Volatile Content of Coatings EPA 24
Water Content Karl Fischer
Microbiological analyses
back to top
Coliform Bacteria, Total and E. Coli SM 9223 B (Presence / Absence)
Coliform Bacteria, Fecal SM 9222 D (Membrane Filtration)
Heterotrophic Plate Count SM 9215 C
E. Coli Hach 10029 (40CFR, Part 141.21)
Mold Phase Contrast Microscopy
Test Matrix Method
References
Organic analyses back to top
Volatile Organics by Gas Chromatography / Mass Spectrometry (GC/MS)
Purgeable Organics Water EPA 624 / 8260
  Soil* EPA 8260
Volatiles (Operational Memo 2) Water EPA 624 / 8260 / 8011 (GSI)
  Soil* EPA 8260
Volatile Organics by Gas Chromatography (GC)
BTEX / MTBE Water  EPA 602 / 8021
  Soil* EPA 8021
Alcohols and Glycols Water EPA 8015 (Modified)
  Soil EPA 8015 (Modified)
Total Petroleum Hydrocarbons - Gasoline Range Organics, (GRO) Water EPA 8015 (Modified)
  Soil* EPA 8015 (Modified)
Methane, Ethane, Ethene Water  TAL Method
Semi-Volatile Organics by Gas Chromatography (GC)
Chlorinated Herbicides Water EPA 515.1 / 8151
Organochlorine Pesticides Water EPA 608 / 8081
  Soil EPA 8081
Polychlorinated Biphenyls, (PCBs) Water EPA 608 / 8082
  Soil EPA 8082
  Oil EPA 8082
Chlorinated Compounds (GSI) Water EPA 8041 / 8121
  Soil EPA 8041 / 8121
Total Petroleum Hydrocarbons - Diesel Range Organics, (DRO) Water EPA 8015 (Modified)
  Soil EPA 8015 (Modified)
Semi-Volatile Organics by High Performance Liquid Chromatography (HPLC)
Polnuclear Aromatic Hydrocarbons, (PNAs) (PAHs) Water EPA 610 / 8310
  Soil EPA 8310
Explosives Water EPA 8330
  Soil EPA 8330
Semi-Volatile Organics by Gas Chromatography / Mass Spectrometry (GS/MS)
Base / Neutral / Acid Fraction, (BNA) Water EPA 8271 / 625
  Soil EPA 8270
Polynuclear Aromatic Hyrdrocarbons, (PNAs) (PAHs) Water EPA 8270 / 625
  Soil EPA 8270
* May require methanol presevation or use of En-Core type sampling device
Air monitoring  back to top
Volatiles by GC/MS (Tedlar Bags) Air Modified 8260
Volatiles by GC/FID (Charcoal Tubes)
A) BTEX
B) Project Specific List
Air Modified NIOSH 1501
Metals Analysis on Filters Air 6010
RCRA waste characterization  back to top
Individual analyses
Corrosivity, PH Liquid EPA 9040
  Solid EPA 9045
Ignitability, Flash Point Solid / Liquid EPA 1010
Paint Filter Test Solid / Liquid EPA 9095
Reactivity, Cyanide and Sulfide Solid / Liquid EPA SW-846, Chapter 7
TCLP Extraction for Metals, Semi-Colatiles, Pesticides and Herbicides Solid / Liquid EPA 1311
TCLP ZHE Extraction for TCLP Volatiles Solid / Liquid EPA 1311
SPLP Extraction for Metals, Semi-Volatiles, Pesticides and Herbicides Solid EPA 1312
SPLP ZHE Extraction for SPLP Volatiles Solid EPA 1312
Metals analyses  back to top
Individual elements
Hexavalent Chromium Water EPA 7196
  Soil EPA 7196
ICP Water EPA 200.7 / 6010
  Soil EPA 6010
ICP/MS Water EPA 200.8 / 6020
  Soil EPA 6020
Mercury, Cold Vapor AA Water  EPA 245.1 / 7470
  Soil  EPA 7471
Low-level Mercury, (CVAF) Water  EPA 1631
Zeeman Graphite Furnance AA Water EPA 200.0 Series / 7000 Series
  Soil EPA 7000 Series
Metals Preparation - Digestion Water EPA 3015
  Soil EPA 3051
Coarse and Fine Lead (Operational Memo 2) Soil MDEQ SOP 213
List metals
RCRA Metals (Arsenic, Barium, Cadmium, Chromium, Lead, Mercury, Selenium, Silver) Water EPA 6000 / 7000 Series
  Soil EPA 6000 / 7000 Series
MDEQ Metals (Same as RCRA Metals plus Copper and Zinc) Water EPA 6000 / 7000 Series
  Soil EPA 6000 / 7000 Series
MDEQ Operation Memo 2 Metals (Antimony, Arsenic, Barium, Cadmium, Cobalt, Copper, Chromium, Iron, Lead**, Mercury, Molybdenum, Nickel, Selenium, Silver, Thallium, Vanadium, Zinc) Water EPA 6000 / 7000 Series
  Soil EPA 6000 / 7000 Series
Target Analyte Metals (Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Vanadium, Zinc) Water EPA 6000 / 7000 Series
  Soil EPA 6000 / 7000 Series
** May require coarse and fine fractions for soil samples.
 

Standard services list

General chemistry parameters

Microbiological analyses

Organic analyses

Air monitoring

RCRA waste characterization

Metals analyses


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Standard services list
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